Dataset of the article with title: Study of the Electrocatalytic Hydrogenation of Benzaldehyde and Furfural at Heterostructured MoS2/N-Carbon Thin-Film Electrodes; Published in ACS Electrochemistry.

DOI of the article: https://doi.org/10.1021/acselectrochem.5c00361

Description of the .txt files in the accompanying data set:

Figure1: Raman Spectra of the MoS2/anC:NG material shown in Figure 1d and zoomed in in 1e.

The Folder 'Figure1 Images' contains the Microscopy images and the Raman heatmap shown in Figure 1.

Figure2 XPS Survey: XPS Survey Spectra for the MoS2/anC:NG material shown in Figure 2a.
Figure2 XPS Mo 3d: XPS spectra for the Mo 3d core level for the MoS2/anC:NG material shown in Figure 2b.
Figure2 XPS S 2p: XPS spectra for the S 2p core level for the MoS2/anC:NG material shown in Figure 2c.
Figure2 CV Loading: Cyclic voltammetry response for the MoS2/anC:NG material used to determine the loading of MoS2 as shown in Figure 2d.

Figure3 LSV: Data series for linear sweep voltammetry measurements on a anC:NG and a MoS2/anC:NG electrode in 0.1M H2SO4 with and without 10mM Benzaldehyde, as shown in Figure 3.

Figure4 Chronoamperometry: Data series for the current response of chronoamperometry experiments on a MoS2/anC:NG electrode at -0.6, -0.7, -0.8, -0.9 and -1.0 V vs. Ag/AgCl, as shown in Figure 4a.
Figure4 KPIs Benzaldehyde: Data series contains the performance indicators for electrolysis experiments on MoS2/anC:NG electrodes in 0.1M H2SO4 with 20mM Benzaldehyde as shown in Figure 4b-f.

Figure5 KPIs Furfural: Data series contains the performance indicators for electrolysis experiments on MoS2/anC:NG electrodes in 0.1M H2SO4 with 20mM Furfural as shown in Figure 5a-d.
